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Overview
Laboratory jacketed glass reactors are temperature-controlled instruments and equipment for cooling and heating functions. Generally speaking, matching reactors, reactors, distillation, extraction, etc. Range and power vary.
The working principle of the laboratory jacketed glass reactor:
put the reaction solvent in the inner layer of the glass for stirring reaction, and the interlayer can be connected to different cold and heat sources (refrigerated liquid, hot water or hot oil) for cyclic heating or cooling reaction. Through the interlayer of the double-layer reaction kettle, a constant temperature (high or low temperature) hot solution medium or cooling medium is injected, and the materials in the reaction kettle are heated or refrigerated at a constant temperature. At the same time, stirring reaction can be carried out under normal pressure or negative pressure according to the requirements of use. The materials are reacted in the reactor, and the evaporation and reflux of the reaction solution can be controlled. After the reaction, the materials can be discharged from the outlet at the bottom of the reactor, which is very convenient to operate.
Laboratory jacketed glass reactor features:
1. The laboratory jacketed glass reactor has a wide temperature control range and a wide temperature control range. Explosion-proof customization services can be provided according to customer requirements.
2. The accessories are all qualified brands, and the controller can be controlled by PLC touch screen and industry-specific single-chip microcomputer according to customer requirements.
3. The heating tubes in the core parts of the electrical and heating systems are all brand-name, equipped with overcooling and overheating protection devices, equipped with industry-specific high and low temperature resistant pumps, and the failure rate is relatively low. The isolated electric control box protects the electrical parts from corrosion and prolongs the use. life.
4. Optional full metal surface frame or stainless steel sheet metal, with a streamlined and beautiful design, to ensure long-term stable cooling and heating operation of the product.
5. The evaporator adopts an internal thread heat exchanger, and the condensation efficiency is higher than that of ordinary heat dissipation.
6. In addition to the functions of over-undervoltage, phase loss, and overload provided by the internal protection module of the compressor, it is also equipped with protection devices such as anti-freezing, overheating, and pressure control to make the unit work more stably.
7. It adopts intelligent control, good stability, high repeatability of results, relatively simple operation when using, equipment models of different sizes, there are different sizes, and it occupies a relatively small area. It can be equipped with one reactor, or it can be equipped with multiple reactors for cooling, heating and temperature control.
8. After commissioning and leaving the factory, component installation, operation commissioning and testing under different working conditions have been completed in the factory, ensuring that each device is qualified to leave the factory, greatly reducing the time for on-site installation and commissioning.
Features
1. GG17 high-borosilicate glass with nice physical-chemical properties; experiment temperature -100 to 400 degree C; Resistant to strong acidic properties of materials; only touching with glass parts & PTFE, no cross-contamination. Double cylinder; kettle cover is separated from kettle body. It is convenient to disassemble, clean and install.
2. Stirring adopts to mechanical sealing, it keeps higher vacuum degree among the same products in the market. It also keeps high vacuum degree when stirring. Glass(PTFE)discharge valve, non-dead angle mixing, fast emptying, no residue.
3. Frequency control speed gear motor, smooth running，high torque, automatic booster, no spark, noise free, long life. SUS frame and cast aluminum material kettle body support, elegant appearance, stable structure.
4. Circulating water/oil bath, high and low temperature machine can supply heating source; Cooling machine:cooling chiller，high and low temperature machine，convenient and practical.
5. Scientific & innovative structure, practical, elegant appearance, domestic industry-leading. Explosion proof is optional.
Precautions for using laboratory jacketed glass reactor:
1. When using vacuum grease on rotating parts such as glass cocks or feeding tubes, please choose a smooth and sticky brand.
2. If the grinding mouth has been fastened or stuck to death, forcibly dismantling it at this time will cause the glass to break, which is very dangerous. When sticking occurs at the grinding mouth, please use heating methods (hot water, blowtorch) to soften the solidified vacuum grease before disassembly.
3. The reaction medium loaded should not exceed 2/3 of the liquid level of the kettle body.
4. When the work is over, it is strictly forbidden to disassemble under pressure! It is strictly forbidden for the reactor to work under overpressure and overtemperature.
Laboratory jacketed glass reactor ancillary equipment:
Circulating water vacuum pump: To provide a vacuum source.
Cool chiller: Low temperature reaction and Re-flux, condensation.
Circulating water/oil bath: Thermal power.
High and low temperature machine: High and low temperature experiment reaction.
Cylindrical Reactor, the liner is for reaction solvent, and the jacket for heating or cooling resource(cool liquid,hot water or hot oil), to achieve circulating heating or cooling experiment. And its ancillary equipment-High and low temperature machine which can satisfy functional high & low temp reaction experiments.
Specifications
Technical Parameter
| Model | (EX)S-10L |
| Power supply | AC220V |
| Stirring power(W ) | 120 1/3 Gear Motor |
| Rotary speed(rpm) | 0~600 |
| Torque(g/cm) | 1000 |
| Capacity(L) | 10 |
| Discharge method | Discharge from bottom, discharge valve |
Detailed technical datas:
| Model | S-10 |
| Shaft diameter | 14mm |
| Stirring neck (flange) | Φ33mm 50mm |
| Thermometer (taper) | 24#*Φ34 |
| Inlet/outlet volume gas (taper) | 34#*Φ45 |
| Solid feeding neck (flange) | Φ60mm 80mm |
| Condensing neck (1-5taper10-100round) | 50#Φ60 |
| Liquid feeding neck（taper） | Φ40mm 50mm |
| Bottom discharge neck（flange） | Glass Φ30mm 70mm |
| Jacket liquid Inlet/Outlet | Φ10mm 20mm |
| Stirrer length,diameter,weight | 720mm Φ200 mm 0.8kg |
| Thermowell length,diameter,weight | 510mm Φ15mm 0.1kg |
| Stirring seal (heitht,diameter,weight, ) | 190mm Φ50mm 0.55kg |
| Funnel (height diameter,weight,) | 490mm Φ84mm 1kg |
| Condenser (length,diameter,weight) | 620mm Φ61mm 1kg |
| Glass Bottom discharge | 210mm Φ160mm |
Tips:
1.Voltage 110V or 380V is available.
2.Stirring power, torgue, refrigeration components can be customized.
3.Cusomized cofiguration is available.